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Structure elucidation and 1H/13C NMR spectral assignments of four trabectedin related compounds
Vermeulen, W.; Filliers, W.; Garcia, C.; Manzanaro, S.; Montalvo, D.; Polanco, C.; Spillemaeckers, F.; Van Hoof, B.; Winderickx, G.; Somers, I.; Rodriguez-Campos, I. (2008). Structure elucidation and 1H/13C NMR spectral assignments of four trabectedin related compounds. Magnetic Resonance in Chemistry 46(12): 1198-1202. dx.doi.org/10.1002/mrc.2334
In: Magnetic Resonance in Chemistry. Wiley-Blackwell: Hoboken. ISSN 0749-1581, more
Peer reviewed article  

Available in  Authors 

Keyword
    Marine
Author keywords
    NMR; H-1; C-13; synthesis; trabectedin; ecteinascidin; Yondelis

Authors  Top 
  • Vermeulen, W.
  • Filliers, W.
  • Garcia, C.
  • Manzanaro, S.
  • Montalvo, D.
  • Polanco, C.
  • Spillemaeckers, F.
  • Van Hoof, B.
  • Winderickx, G.
  • Somers, I.
  • Rodriguez-Campos, I.

Abstract
    This article presents the structure elucidation of four new compounds, formed during the hemisynthetic preparation of trabectedin, an anti-tumor natural product from Ecteinascidia turbinata. We report herein on the use of UV, MS and NMR spectroscopic data along with 1H and 13C spectral assignments obtained by means of 1D and 2D homo- and heteronuclear NMR techniques.

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