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Determination of methylmercury in natural waters by headspace gas chromatography with microwave-induced plasma detection after preconcentration on a resin containing dithiocarbamate groupsPeer reviewed article
Lansens, P.; Meuleman, C.; Leermakers, M.; Baeyens, W.F.J. (1990). Determination of methylmercury in natural waters by headspace gas chromatography with microwave-induced plasma detection after preconcentration on a resin containing dithiocarbamate groups Anal. Chim. Acta 234: 417-424
In: Analytica Chimica Acta. Elsevier: Amsterdam. ISSN 0003-2670, meer

Ook gepubliceerd als
  • Lansens, P.; Meuleman, C.; Leermakers, M.; Baeyens, W.F.J. (1990). Determination of methylmercury in natural waters by headspace gas chromatography with microwave-induced plasma detection after preconcentration on a resin containing dithiocarbamate groups, in: (1990). IZWO Coll. Rep. 20(1990). IZWO Collected Reprints, 20: pp. chapter 28 [Subsequent publication], meer

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Abstract
    A method for the determination of methylmercury at ng 1-1 levels in natural waters is described. Methylmercury present in a sample is first preconcentrated on a column of a resin containing dithiocarbamate groups and eluted quantitatively with acidic thiourea solution. Methylmercury in the effluent is then converted to the iodide by addition of sulphuric acid and iodoacetic acid and determined by headspace gas chromatography with microwave-induced plasma detection. The adsorption properties of the resin are discussed.

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